| Issue |
E3S Web Conf.
Volume 497, 2024
5th International Conference on Energetics, Civil and Agricultural Engineering (ICECAE 2024)
|
|
|---|---|---|
| Article Number | 03030 | |
| Number of page(s) | 6 | |
| Section | Agricultural Engineering | |
| DOI | https://doi.org/10.1051/e3sconf/202449703030 | |
| Published online | 07 March 2024 | |
Chemical technology of oligomers production from homopolymer based on epichlorohydrin and morpholine
Tashkent State Technical University named after Islam Karimov, Tashkent, 100095, Uzbekistan.
* Corresponding author: u.urinov@tdtu.uz
In this paper, the effect of different solvents on the spontaneous polymerization reaction of morpholine and epichlorohydrin is studied. Also. The reaction have been established: factors temperature, proportions of initial substances, optimal values of such parameters as temperature.On the basis of the developed technology the yield of oligomeric product with epichlorohydrin based on morpholine 92-95% was determined. The structure of the synthesized oligomeric substance was established by spectral methods, IR, PMR spectroscopy.The technological scheme for the preparation of polymer products based on 3-chloro-1-morpholyl-2-isopropylacrylate was also developed and the influence of reaction time, temperature and ratio of initial substances on the process was studied. Preparation of oligomer based on morpholine with epichlorohydrin.Processes and technology for obtaining homopolymers based on 3-chloro-1-morpholyl-2-isopropylacrylate were developed.
© The Authors, published by EDP Sciences, 2024
This is an Open Access article distributed under the terms of the Creative Commons Attribution License 4.0, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.
Current usage metrics show cumulative count of Article Views (full-text article views including HTML views, PDF and ePub downloads, according to the available data) and Abstracts Views on Vision4Press platform.
Data correspond to usage on the plateform after 2015. The current usage metrics is available 48-96 hours after online publication and is updated daily on week days.
Initial download of the metrics may take a while.