E3S Web Conf.
Volume 252, 20212021 International Conference on Power Grid System and Green Energy (PGSGE 2021)
|Number of page(s)||5|
|Section||Research and Development of Electrical Equipment and Energy Nuclear Power Devices|
|Published online||23 April 2021|
Study on novel structure of tris-(4,4′-dimethyl-2,2′-dipyridyl) Nickel salicylic acid boric acid, Ni(C12H12N2)3●(C7H5O3)2●(H3BO3)
1 Department of Chemical Engineering, Weifang Vocational College, Weifang 262737, China
2 Chemistry & Chemical & Environmental Engineering College, Weifang University, Weifang 261061, China
* Corresponding author: email@example.com
A novel complex Ni(C12H12N2)3●(C7H5O3)2●(H3BO3) has been synthesized from a hydrothermal reaction and the crystal structure has been determined by means of single-crystal X-ray diffraction. Triclinic, P-1. a= 12.5380(13) Å, b = 13.0100(15) Å, c = 15.1490(18) Å, α= 102.760(3)°, β= 94.480(2)°, γ= 94.540(2)°. V=2390.9(5) Å3. Z=2. R1 =0.0661, wR2 = 0.2128, T=293(2) K. The Ni atom is coordinated by six N atoms from three 4,4′-dimethyl-2,2′-dipyridyl molecular. The molecular structure stabilized by the O-H…O hydrogen-bonding interactions.
© The Authors, published by EDP Sciences, 2021
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